Metabolomics Society Forum

Hardware => Mass spectrometers => Topic started by: hwhitwell on April 03, 2016, 05:24:15 AM

Title: LQT Convectron gauge pressure too high.
Post by: hwhitwell on April 03, 2016, 05:24:15 AM
Hello,

I am running an LTQ-Orbitrap XL and have high pressure (2.4 and should be 1) on the convectron gauge for the LTQ. I removed the ion tube to block the ion inlet to the front of the API stack, the vacuum should drop to zero, but only achieves 0.2, therefore I think there must be a leak somewhere between the API stack and the vacuum pumps.

I have tried dripping some methanol around to API stack whilst watching the vacuum levels on the convectron gauge, however I couldn't find anywhere...

If I put my ear to the the panel below the API stack I can hear a small hiss, but I don't know if it is related or not...!

Has anyone had any similar problems or can anyone suggest something to check?

Thanks!